| 1315192-62-1

• 分子结构分类: 有机化合物 - 有机氧化合物
• CAS: 1315192-62-1
• 化学式: C₇₇H₉₁N₃O₁₇
• 分子量: 1330.58
• InChiKey: WUBZBJRYKJSSSX-NGZLPZTMSA-N

反应信息

• 作为反应物：
  描述：

  在 palladium 10% on activated carbon 、 氢气 作用下， 以 四氢呋喃 、 甲醇 为溶剂， 反应 24.0h， 生成
  参考文献：
  名称：

  Concise synthesis of Bacillus anthracis exosporium tetrasaccharide via two-stage activation of allyl glycosyl donor strategy

  摘要：

  A highly efficient glycosylation protocol recently developed in our laboratory has been utilized in the short synthesis of the tetrasaccharide 1, an antigen important to the development of carbohydrate-based diagnostic tools and vaccines against anthrax. The protocol employs allyl glycosides as building blocks and improves the overall synthetic efficiency. (C) 2011 Elsevier Ltd. All rights reserved.

  DOI：

  10.1016/j.tetlet.2011.05.089
• 作为产物：
  描述：

  在 9λ²-borabicyclo[3.3.1]nonane 、 双氧水 、 sodium hydroxide 作用下， 以 四氢呋喃 为溶剂， 反应 15.5h， 以87%的产率得到
  参考文献：
  名称：

  Concise synthesis of Bacillus anthracis exosporium tetrasaccharide via two-stage activation of allyl glycosyl donor strategy

  摘要：

  A highly efficient glycosylation protocol recently developed in our laboratory has been utilized in the short synthesis of the tetrasaccharide 1, an antigen important to the development of carbohydrate-based diagnostic tools and vaccines against anthrax. The protocol employs allyl glycosides as building blocks and improves the overall synthetic efficiency. (C) 2011 Elsevier Ltd. All rights reserved.

  DOI：

  10.1016/j.tetlet.2011.05.089