| 957220-39-2

• 分子结构分类: 有机化合物 - 有机杂环化合物 - 喹啉及其衍生物
• CAS: 957220-39-2
• 化学式: C₁₄H₁₃Cl₂N
• 分子量: 266.17
• InChiKey: GIMRUPYDCJQGGS-UHFFFAOYSA-N

反应信息

• 作为反应物：
  描述：

  在 sodium hydroxide 、 硫酸 作用下， 以 丙酮 为溶剂， 反应 1.5h， 生成 2,4,6-trimethylthieno[3,2-c]quinoline
  参考文献：
  名称：

  Synthesis of substituted 2,4-dimethylthieno[3,2-c]quinolines

  摘要：

  A procedure was developed for the synthesis of substituted 2,4-dimethylthieno[3,2-c]quinolines via intramolecular cyclization and subsequent arornatization of 3-(2-chloroprop-2-en-1-yl)- and 3-(2-oxopropyl)-2methylquinoline-4-thiols. The latter were obtained by alkaline hydrolysis of the corresponding thiuroniurn salts which were prepared in turn by reactions of 4-chloro-3-(2-chloroprop-2-en-1-yi)- and 4-chloro-3-(2-oxopropyl)-2-methylquinolines with thiourea.

  DOI：

  10.1134/s1070428007030165
• 作为产物：
  描述：

  在 三氯氧磷 作用下， 生成
  参考文献：
  名称：

  Synthesis of substituted 2,4-dimethylthieno[3,2-c]quinolines

  摘要：

  A procedure was developed for the synthesis of substituted 2,4-dimethylthieno[3,2-c]quinolines via intramolecular cyclization and subsequent arornatization of 3-(2-chloroprop-2-en-1-yl)- and 3-(2-oxopropyl)-2methylquinoline-4-thiols. The latter were obtained by alkaline hydrolysis of the corresponding thiuroniurn salts which were prepared in turn by reactions of 4-chloro-3-(2-chloroprop-2-en-1-yi)- and 4-chloro-3-(2-oxopropyl)-2-methylquinolines with thiourea.

  DOI：

  10.1134/s1070428007030165