1-phenanthridin-6-yl-2-p-tolylethane-1,2-dione | 1336885-59-6

• 分子结构分类: 有机化合物 - 有机杂环化合物 - 喹啉及其衍生物
• 英文名称: 1-phenanthridin-6-yl-2-p-tolylethane-1,2-dione
• CAS: 1336885-59-6
• 化学式: C₂₂H₁₅NO₂
• 分子量: 325.367
• InChiKey: VVMPJCLVMHXVGE-UHFFFAOYSA-N

反应信息

• 作为产物：
  描述：

  在 水 、 碘 、 sodium dodecyl-sulfate 作用下， 反应 0.58h， 以81%的产率得到1-phenanthridin-6-yl-2-p-tolylethane-1,2-dione
  参考文献：
  名称：

  Ultrasound-assisted synthesis of aromatic 1,2-diketones from oximinoketones under neutral conditions in aqueous media

  摘要：

  We report a convenient, neutral, and facile methodology for the synthesis of aromatic 1,2-diketones from the corresponding oximinoketones in the presence of I-2/SDS/water system under ultrasound-assisted conditions. Furthermore, a series of compounds were synthesized and characterized by melting point, IR, NMR, MS, and elemental analysis. Utilization of easy reaction conditions, very high to excellent yields, and short reaction times makes this manipulation potentially very useful. (C) 2011 Elsevier B.V. All rights reserved.

  DOI：

  10.1016/j.ultsonch.2011.05.011