2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9,9-bis[3-ethoxycarbonyl-4-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]phenyl]-fluorene | 1250437-63-8

• 分子结构分类: 有机化合物 - 苯类化合物 - 芴
• 英文名称: 2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9,9-bis[3-ethoxycarbonyl-4-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]phenyl]-fluorene
• 英文别名: 2,7-Bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9,9-bis[3-ethoxycarbonyl-4-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]phenyl]-fluorene；ethyl 5-[9-[3-ethoxycarbonyl-4-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]phenyl]-2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)fluoren-9-yl]-2-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzoate
• CAS: 1250437-63-8
• 化学式: C₅₇H₇₆B₂O₁₆
• 分子量: 1038.84
• InChiKey: MGWDUSCBPBFSLV-UHFFFAOYSA-N

计算性质

• 辛醇/水分配系数(LogP)：
  7.12
• 重原子数：
  75
• 可旋转键数：
  30
• 环数：
  7.0
• sp3杂化的碳原子比例：
  0.54
• 拓扑面积：
  163
• 氢给体数：
  0
• 氢受体数：
  16

反应信息

• 作为反应物：
  描述：

  2,7-dibromo-9,9-bis[3-ethoxycarbonyl-4-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]phenyl]-fluorene 、 2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9,9-bis[3-ethoxycarbonyl-4-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]phenyl]-fluorene 、 、 disodium;carbonate 、 4-叔丁基苯硼酸 、 sodium N,N-diethyldithiocarbamate 、 在 甲基三辛基氯化铵 四氢呋喃 、 silica gel 、 甲醇 作用下， 以 四氢呋喃 、 甲醇 、 溶剂黄146 、 甲苯 为溶剂， 反应 20.5h， 生成 9,9-Bis[3-ethoxycarbonyl-4-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]phenyl]-fluorene
  参考文献：
  名称：

  METHOD FOR MANUFACTURING ORGANIC ELECTROLUMINESCENT ELEMENT

  摘要：

  一种制造有机电致发光元件的方法，包括以下顺序的部分：阳极、发光层、电子注入层和阴极。该方法包括以下步骤：（A）形成阳极；（B）形成发光层；（C）形成电子注入层；（D）形成阴极。其中步骤（C）包括（i）涂布含有离子聚合物的应用液体以形成薄膜，（ii）加热所形成的薄膜，（iii）存储部分完成的有机电致发光元件并随后（iv）再次加热薄膜。

  公开号：

  US20130323871A1

文献信息

• Method for manufacturing organic light-emitting device and organic light-emitting device
  申请人：Sassa Shuichi

  公开号：US08963422B2

  公开（公告）日：2015-02-24

  The present invention provides a method for manufacturing an organic light-emitting device capable of simply manufacturing the organic light-emitting device without requiring a vacuum atmosphere. The manufacturing method of the present invention includes: a step of preparing a supporting substrate having an organic electroluminescent element formed thereon, the organic electroluminescent element containing an anode, a light-emitting layer, an electron injection layer made by forming a film with a solution containing an ionic polymer, and a cathode; and a step of laminating the supporting substrate and a sealing member to one another so as to seal the organic electroluminescent element.

  本发明提供了一种制造有机发光器件的方法，该方法能够简单地制造有机发光器件，而不需要真空气氛。本发明的制造方法包括：准备一个支撑基板，该支撑基板上形成有一个有机电致发光元件，该有机电致发光元件包含一个阳极、一个发光层、一个由含有离子聚合物的溶液形成的电子注入层和一个阴极；以及将支撑基板和密封件层压在一起，以密封有机电致发光元件。
• METHOD FOR MANUFACTURING ORGANIC LIGHT-EMITTING DEVICE AND ORGANIC LIGHT-EMITTING DEVICE
  申请人：Sassa Shuichi

  公开号：US20130112966A1

  公开（公告）日：2013-05-09

  The present invention provides a method for manufacturing an organic light-emitting device capable of simply manufacturing the organic light-emitting device without requiring a vacuum atmosphere. The manufacturing method of the present invention includes: a step of preparing a supporting substrate having an organic electroluminescent element formed thereon, the organic electroluminescent element containing an anode, a light-emitting layer, an electron injection layer made by forming a film with a solution containing an ionic polymer, and a cathode; and a step of laminating the supporting substrate and a sealing member to one another so as to seal the organic electroluminescent element.

  本发明提供了一种制造有机发光器件的方法，能够简单地制造有机发光器件而不需要真空气氛。本发明的制造方法包括以下步骤：准备一个支撑基板，在其上形成有机电致发光元件，该有机电致发光元件包含阳极、发光层、通过使用含有离子聚合物的溶液形成薄膜的电子注入层和阴极；将支撑基板和密封件层叠在一起，以密封有机电致发光元件。
• Method for manufacturing organic electroluminescent element
  申请人：Sassa Shuichi

  公开号：US09006008B2

  公开（公告）日：2015-04-14

  A method for manufacturing an organic electroluminescent element including, in the following order, an anode, a light-emitting layer, an electron injection layer, and a cathode, the method including the steps of: (A) forming the anode; (B) forming the light-emitting layer; (C) forming the electron injection layer; and (D) forming the cathode, in which the step (C) includes (i) applying an application liquid containing an ionic polymer to form a thin film, (ii) heating the thin film formed, (iii) storing a partially finished organic electroluminescent element obtained in (ii), and thereafter, (iv) heating the thin film again.

  一种制造有机电致发光元件的方法，包括以下顺序的元素：阳极、发光层、电子注入层和阴极，该方法包括以下步骤：（A）形成阳极；（B）形成发光层；（C）形成电子注入层；和（D）形成阴极，其中步骤（C）包括（i）涂布含有离子聚合物的应用液体以形成薄膜，（ii）加热所形成的薄膜，（iii）存储部分完成的有机电致发光元件，然后（iv）再次加热所形成的薄膜。
• METHOD FOR MANUFACTURING ORGANIC ELECTROLUMINESCENT ELEMENT
  申请人：Sassa Shuichi

  公开号：US20130323871A1

  公开（公告）日：2013-12-05

  A method for manufacturing an organic electroluminescent element including, in the following order, an anode, a light-emitting layer, an electron injection layer, and a cathode, the method including the steps of: (A) forming the anode; (B) forming the light-emitting layer; (C) forming the electron injection layer; and (D) forming the cathode, in which the step (C) includes (i) applying an application liquid containing an ionic polymer to form a thin film, (ii) heating the thin film formed, (iii) storing a partially finished organic electroluminescent element obtained in (ii), and thereafter, (iv) heating the thin film again.

  一种制造有机电致发光元件的方法，包括以下顺序的部分：阳极、发光层、电子注入层和阴极。该方法包括以下步骤：（A）形成阳极；（B）形成发光层；（C）形成电子注入层；（D）形成阴极。其中步骤（C）包括（i）涂布含有离子聚合物的应用液体以形成薄膜，（ii）加热所形成的薄膜，（iii）存储部分完成的有机电致发光元件并随后（iv）再次加热薄膜。