The present invention relates to a method for producing an oligonucleic acid compound, the method being characterized by (1) treating a compound represented by formula [A-1] and a compound represented by formula [B-1] with a condensation agent in the presence of a base and then (2) treating the compounds with an oxidizing agent and an organic amine to produce a compound represented by formula [C-1] (in the formulae, each symbol is as defined in the description).
A grease composition is produced by mixing a thickener of a calcium sulfonate complex and a second thickener component (polyurea, a metallic soap, a complex metallic soap or an N-substituted terephthalamic acid metal salt) into a base oil. This grease composition is excellent in heat resistance, load carrying capacity, water resistance and lubricating life.
Moreover, a grease composition is produced by mixing a thickener of an N-substituted terephthalamic acid metal salt and a second thickener component (polyurea, a metallic soap or a complex metallic soap) into a base oil. This grease composition is excellent in heat resistance, oxidation stability and lubricating life.
Furthermore, a grease composition is produced by mixing a thickener of 10 to 90% by mass of polyurea and 90 to 10% by mass of a complex metallic soap into an ester oil having a kinematic viscosity at 40° C. of 20 to 180 mm
2
/s. This grease composition generates only a few dusts even at a high temperature and has excellent high-temperature performance.
Still further, a grease composition is produced by mixing a thickener of 10 to 90% by mass of polyurea and 90 to 10% by mass of a complex metallic soap into a base oil having a kinematic viscosity at 40° C. of 50 to 500 mm
2
/s. This grease composition has excellent performance under a high-speed and high-temperature environment and provides a rolling apparatus with excellent seizuring life.