Darstellung und Kristallstruktur von P4O8 / Preparation and Crystal Structure of P4O8
作者:Stephan Strojek、Martin Jansen
DOI:10.1515/znb-1997-0804
日期:1997.8.1
Abstract P4O8 was synthesized for the first time in a pure state. Its crystal structure has been refined using X-ray diffractometer data (monoclinic, C2/c with a = 970.0(2); b = 1017.9(2); c = 692.3(1) pm; β = 96.95(2)°; V = 678.5 Å3; R1 = 0.033; wR2 = 0.073). Molecular geometry and packing in the solid state are discussed.
摘要 P4O8 是首次以纯态合成。其晶体结构已使用 X 射线衍射仪数据(单斜晶系,C2/c,a = 970.0(2); b = 1017.9(2); c = 692.3(1) pm; β = 96.95(2)°; V = 678.5 Å3;R1 = 0.033;wR2 = 0.073)。讨论了固态分子的几何形状和堆积。