ethyl 2-oxo-4-phenyl-6-((2-phenylhydrazinyl)methyl)-1,2-dihydropyrimidine-5-carboxylate | 1158956-11-6

• 分子结构分类: 有机化合物 - 有机杂环化合物 - 二嗪类
• 英文名称: ethyl 2-oxo-4-phenyl-6-((2-phenylhydrazinyl)methyl)-1,2-dihydropyrimidine-5-carboxylate
• CAS: 1158956-11-6
• 化学式: C₂₀H₂₀N₄O₃
• 分子量: 364.404
• InChiKey: MZHCCKUURUHKJS-UHFFFAOYSA-N

物化性质

• 密度：
  1.26±0.1 g/cm3(Temp: 20 °C; Press: 760 Torr)(predicted)

反应信息

• 作为反应物：
  描述：

  ethyl 2-oxo-4-phenyl-6-((2-phenylhydrazinyl)methyl)-1,2-dihydropyrimidine-5-carboxylate 以 乙酰乙酸乙酯 为溶剂， 反应 3.0h， 以79%的产率得到4,6-diphenyl-1H-pyrimido[4,5-d]pyridazine-2,5-(1H,6H)-dione
  参考文献：
  名称：

  A Convenient Route to New Pyrrolo[1,2-c]pyrimidone, Thiazolo[3,4-c]pyrimidone and Pyrimido[4,5-d]pyridazine Derivatives

  摘要：

  The utility of versatile, readily accessible ethyl 6-bromomethyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate (3) and ethyl 6-bromomethyl-2-oxo-4-phenyl-1,2-dihydropyrimidine-5-carboxylate (4) in the synthesis of some new pyrimidine, pyrimido[4,5-d]pyridazine, pyrrolo[1,2-c]pyrimidone and thiazolo[3,4-c]pyrimidone derivatives is reported.

  DOI：

  10.3987/com-08-11562
• 作为产物：
  描述：

  ethyl 6-(bromomethyl)-1,2-dihydro-2-oxo-4-phenylpyrimidine-5-carboxylate 、 苯肼 以 乙醇 为溶剂， 反应 4.0h， 以79%的产率得到ethyl 2-oxo-4-phenyl-6-((2-phenylhydrazinyl)methyl)-1,2-dihydropyrimidine-5-carboxylate
  参考文献：
  名称：

  A Convenient Route to New Pyrrolo[1,2-c]pyrimidone, Thiazolo[3,4-c]pyrimidone and Pyrimido[4,5-d]pyridazine Derivatives

  摘要：

  The utility of versatile, readily accessible ethyl 6-bromomethyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate (3) and ethyl 6-bromomethyl-2-oxo-4-phenyl-1,2-dihydropyrimidine-5-carboxylate (4) in the synthesis of some new pyrimidine, pyrimido[4,5-d]pyridazine, pyrrolo[1,2-c]pyrimidone and thiazolo[3,4-c]pyrimidone derivatives is reported.

  DOI：

  10.3987/com-08-11562