Ethyl-4-(4-hydroxyphenyl)-6-methyl-2-thioxo-pyrimidine-5-carboxylate | 1417448-83-9

• 分子结构分类: 有机化合物 - 有机杂环化合物 - 二嗪类
• 英文名称: Ethyl-4-(4-hydroxyphenyl)-6-methyl-2-thioxo-pyrimidine-5-carboxylate
• CAS: 1417448-83-9
• 化学式: C₁₄H₁₄N₂O₃S
• 分子量: 290.343
• InChiKey: GLWKTHWTYVIBCF-UHFFFAOYSA-N

反应信息

• 作为产物：
  描述：

  5-ethoxycarbonyl-6-methyl-4-(4-hydroxyphenyl)-3,4-dihydropyrimidin-2(1H)-thione 以 二甲基亚砜 为溶剂， 反应 0.1h， 以76%的产率得到Ethyl-4-(4-hydroxyphenyl)-6-methyl-2-thioxo-pyrimidine-5-carboxylate
  参考文献：
  名称：

  Facile aromatization of 3,4-dihydropyrimidin-2(1H)-ones (DHPMs) by iodine

  摘要：

  A facile aromatization of 3,4-dihydropyrimidin-2(1H)-ones using iodine in dimethyl sulfoxide under microwave irradiation was carried out which is more efficient and gives high yield in less time; presently it is the most important catalyst for dehydrogenation. (C) 2012 Manisha M. Kodape. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.

  DOI：

  10.1016/j.cclet.2012.10.015