申请人:Iuchi Seiji
公开号:US10350569B2
公开(公告)日:2019-07-16
An object of the present invention is to provide a technique for producing a microcapsule containing a pesticidal compound in a fatty acid ester such as methyl O-acetylricinoleate, which delays the release timing of the pesticidal compound as compared to a conventional microcapsule. Provided is a method for producing a microcapsule, which comprises:
(1) keeping a mixture of a pesticidal compound, a compound represented by formula (I):
wherein X represents —CH2—CH2— or —CH═CH—, R1 represents a C1-C4 alkyl group, and R2 represents a C1-C4 alkyl group, and a polyisocyanate at 20 to 60° C. for 3 hours or more;
(2) adding the mixture to water containing a polyol or a polyamine to prepare liquid droplets in the water; and
(3) forming a film of polyurethane or polyurea around the droplets.
本发明的目的是提供一种生产微胶囊的技术,该微胶囊含有一种脂肪酸酯,如 O-乙酰基蓖麻油酸甲酯中的杀虫化合物,与传统的微胶囊相比,该微胶囊可延长杀虫化合物的释放时间。本发明提供了一种生产微胶囊的方法,其中包括:
(1) 保存杀虫化合物、由式 (I) 代表的化合物的混合物:
其中 X 代表-CH2-CH2-或-CH═CH-,R1 代表 C1-C4 烷基,R2 代表 C1-C4 烷基,以及聚异氰酸酯在 20 至 60 摄氏度的条件下 3 小时或更长时间;
(2) 将混合物加入含有多元醇或多胺的水中,在水中制备液滴;以及
(3) 在液滴周围形成一层聚氨酯或聚脲薄膜。