2-benzoylpyridine nicotinoyl hydrazone

• 分子结构分类: 有机化合物 - 有机杂环化合物 - 吡啶及其衍生物
• 英文名称: 2-benzoylpyridine nicotinoyl hydrazone
• 英文别名: N-[(Z)-[phenyl(pyridin-2-yl)methylidene]amino]pyridine-3-carboxamide
• 化学式: C₁₈H₁₄N₄O
• 分子量: 302.335
• InChiKey: SDBKTVVUMWBZBR-FXBPSFAMSA-N

计算性质

• 辛醇/水分配系数(LogP)：
  2.9
• 重原子数：
  23
• 可旋转键数：
  4
• 环数：
  3.0
• sp3杂化的碳原子比例：
  0.0
• 拓扑面积：
  67.2
• 氢给体数：
  1
• 氢受体数：
  4

反应信息

• 作为产物：
  描述：

  3-吡啶甲酰肼 、 2-苯甲酰吡啶 在 溶剂黄146 作用下， 以 乙醇 为溶剂， 反应 6.0h， 以52%的产率得到2-benzoylpyridine nicotinoyl hydrazone
  参考文献：
  名称：

  Spectral characterization and crystal structure of 2-benzoylpyridine nicotinoyl hydrazone

  摘要：

  The synthesis, spectral characterization and crystal structure of 2-benzoylpyridine nicotinoyl hydrazone (HL) is reported. Spectral techniques employed include H-1 NMR, COSY homonuclear, HSQC heteronuclear correlation techniques, electronic and IR. The infrared spectrum suggests the existence of the compound in keto form in solid state, which is further established by the single crystal X-ray analysis. The compound crystallizes into a triclinic lattice with P-1 symmetry with two molecules per unit cell. (c) 2006 Elsevier B.V. All rights reserved.

  DOI：

  10.1016/j.saa.2006.03.003

文献信息

• Spectral characterization and crystal structure of 2-benzoylpyridine nicotinoyl hydrazone
  作者：Mini Kuriakose、M.R. Prathapachandra Kurup、E. Suresh

  DOI：10.1016/j.saa.2006.03.003

  日期：2007.2

  The synthesis, spectral characterization and crystal structure of 2-benzoylpyridine nicotinoyl hydrazone (HL) is reported. Spectral techniques employed include H-1 NMR, COSY homonuclear, HSQC heteronuclear correlation techniques, electronic and IR. The infrared spectrum suggests the existence of the compound in keto form in solid state, which is further established by the single crystal X-ray analysis. The compound crystallizes into a triclinic lattice with P-1 symmetry with two molecules per unit cell. (c) 2006 Elsevier B.V. All rights reserved.