N-ethyl-N-phenyldiazenylethanamine | 13056-98-9

• 分子结构分类: 有机化合物 - 苯类化合物 - 苯和取代衍生物
• 英文名称: N-ethyl-N-phenyldiazenylethanamine
• 英文别名: 3,3-diethyl-1-phenyltriazene
• CAS: 13056-98-9
• 化学式: C₁₀H₁₅N₃
• 分子量: 177.249
• InChiKey: JHPQXSWFRNIFCC-VAWYXSNFSA-N

物化性质

• 沸点：
  299.18°C (rough estimate)
• 密度：
  1.0940 (rough estimate)

计算性质

• 辛醇/水分配系数(LogP)：
  3.03
• 重原子数：
  13.0
• 可旋转键数：
  4.0
• 环数：
  1.0
• sp3杂化的碳原子比例：
  0.4
• 拓扑面积：
  27.96
• 氢给体数：
  0.0
• 氢受体数：
  2.0

安全信息

• 海关编码：
  2928000090

反应信息

• 作为反应物：
  描述：

  N-ethyl-N-phenyldiazenylethanamine 以63%的产率得到
  参考文献：
  名称：

  SMITH, WILLIAM B.;HO, OLIVER CHENPU, J. ORG. CHEM., 55,(1990) N, C. 2543-2545

  摘要：

  DOI：
• 作为产物：
  描述：

  二乙胺 、 alkaline earth salt of/the/ methylsulfuric acid 以 水 为溶剂， 反应 0.17h， 以83%的产率得到N-ethyl-N-phenyldiazenylethanamine
  参考文献：
  名称：

  在温和条件下使用芳基重氮硫酸硅硫酸盐合成三氮烯

  摘要：

  在本文中描述了一种通过使用芳基重氮氧化硅硫酸盐和仲胺来合成芳基三氮烯的有效，快速和简单的方法。使用本发明的方法，含有吸电子基团和给电子基团的不同种类的芳基重氮氧化硅硫酸盐可以快速地转化为相应的芳基三氮烯，产率高且反应时间短。这些反应是在室温，温和和非均质条件下于水中进行的。此外，对1-（2-硝基苯基）-3,3-二乙基三氮烯进行了温度依赖性NMR光谱研究，以确定该分子N（2）–N（3）键周围的旋转势垒能。该方法的优点是后处理简单，清洁，反应时间短，产率高。

  DOI：

  10.1016/j.dyepig.2013.10.022

文献信息

• The controllable C2 arylation and C3 diazenylation of indoles with aryltriazenes under ambient conditions
  作者：Yonghong Liu、Xia Ma、Gengxin Wu、Ziran Liu、Xiang Yang、Bin Wang、Chenjiang Liu、Yonghong Zhang、Yan Huang

  DOI：10.1039/c9nj01728c

  日期：——

  The controllable C2 arylation and C3 diazenylation of indoles with aryltriazenes under ambient conditions was investigated.

  对苯基三氮烯与吲哚在常温条件下的可控C2芳基化和C3重氮化进行了研究。
• Potential of several triazene derivatives against DENGUE viruses
  作者：Seynabou Sokhna、Natacha Mérindol、Marc Presset、Insa Seck、Marie-Pierre Girard、Seydou Ka、Samba Fama Ndoye、Aïcha Lalla Ba、Issa Samb、Lionel Berthoux、Erwan Le Gall、Isabel Desgagné-Penix、Matar Seck

  DOI：10.1016/j.bmcl.2024.129646

  日期：2024.3

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• Photoresist composition
  申请人：JAPAN SYNTHETIC RUBBER CO., LTD.

  公开号：EP0068808A2

  公开（公告）日：1983-01-05

  By adding a compound of formula (I) or (II): (in which R'-R" are the same or different and each represents a hydrogen atom or an alkyl group) to a conventional photoresist composition comprising a cyclized product of a conjugated diene polymer (which may be a homopolymer or a copolymer) and a photocrosslinking agent soluble in an organic solvent, an image having a high degree of resolution can be obtained. even when a base board having a highly reflecting surface is used, with a high degree of reproducibility and without being affected by prebaking conditions.

  将式（I）或（II）化合物（其中 R'-R" 相同或不同，且各代表氢原子或烷基）添加到由共轭二烯聚合物（可以是均聚物或共聚物）的环化产物和可溶于有机溶剂的光交联剂组成的传统光刻胶组合物中，即使在使用具有高反射表面的基板时，也能获得具有高分辨率的图像，而且重现性高，不受预烘烤条件的影响。
• Ferroelectric liquid crystal composition, liquid crystal optical device produced by using the ferroelectric liquid crystal composition, and method of producing the liquid crystal optical device
  申请人：IDEMITSU KOSAN COMPANY LIMITED

  公开号：EP0352637A2

  公开（公告）日：1990-01-31

  A ferroelectric liquid crystal composition comprising (A) a ferroelectric liquid crystal material and (B) a non-liquid-crystalline polymeric material; a liquid crystal optical device comprising a layer of the ferroelectric liquid crystal composition, the (A) ferroelectric liquid crystal material in the ferroelectric liquid crystal composition has been uniaxially oriented and two substrates which support the layer of the ferroelectric liquid crystal composition between them and carry on their surfaces facing each other their respective electrode layers, at least one of the electrode layers being a transparent electrode layer; and a method of producing the liquid crystal optical device, which method comprises orienting a liquid crystal optical device yet to be oriented which includes a layer of the ferroelectric liquid crystal composition and two flexible substrates which support the layer of the ferroelectric liquid crystal composition between them and carry on their surfaces facing each other their respective electrode layers, by subjecting the liquid crystal optical device yet to be oriented to a bending treatment.

  一种铁电液晶组合物，包括 (A) 铁电液晶材料和 (B) 非液晶聚合物材料； 一种液晶光学器件，包括 一层铁电液晶组合物，铁电液晶组合物中的 (A) 铁电液晶材料已被单轴取向，以及 两个基底，它们 在它们之间支撑着一层铁电液晶组合物，并且 在它们面对面的表面上带有各自的电极层，其中至少一个电极层是透明电极层；以及 一种生产液晶光学器件的方法，该方法包括定向尚未定向的液晶光学器件，该器件包括 一层铁电液晶组合物和 两块柔性基板，它们 在它们之间支撑铁电液晶成分层，并且 在它们面对面的表面上有各自的电极层、 将待定向液晶光学器件进行弯曲处理。
• Method for manufacturing semiconductor device including heating and pressuring a laminate having an adhesive layer
  申请人：HITACHI CHEMICAL COMPANY, LTD.

  公开号：US10669454B2

  公开（公告）日：2020-06-02

  Disclosed is a method for manufacturing a semiconductor device which includes: a semiconductor chip; a substrate and/or another semiconductor chip; and an adhesive layer interposed therebetween. This method comprises the steps of: heating and pressuring a laminate having: the semiconductor chip; the substrate; the another semiconductor chip or a semiconductor wafer; and the adhesive layer by interposing the laminate with pressing members for temporary press-bonding to thereby temporarily press-bond the substrate and the another semiconductor chip or the semiconductor wafer to the semiconductor chip; and heating and pressuring the laminate by interposing the laminate with pressing members for main press-bonding, which are separately prepared from the pressing members for temporary press-bonding, to thereby electrically connect a connection portion of the semiconductor chip and a connection portion of the substrate or the another semiconductor chip.

  本发明公开了一种制造半导体器件的方法，该器件包括：半导体芯片；基板和/或另一个半导体芯片；以及夹在其间的粘合剂层。该方法包括以下步骤：加热和加压层压板，该层压板具有半导体芯片；基板；另一半导体芯片或半导体晶片；以及粘合剂层，将层压板与用于临时加压粘合的加压构件相间，从而将基板和另一半导体芯片或半导体晶片临时加压粘合到半导体芯片上；以及加热和加压层压板，将层压板与用于主加压粘合的加压构件相间，这些加压构件是与用于临时加压粘合的加压构件分开准备的，从而将半导体芯片的连接部分与基板或另一半导体芯片的连接部分电连接起来。