| 1208231-84-8

• 分子结构分类: 有机化合物 - 有机杂环化合物 - 二嗪类
• CAS: 1208231-84-8
• 化学式: C₁₅H₁₇N₃OS
• 分子量: 287.385
• InChiKey: LPCBQQQEQIIYSF-UHFFFAOYSA-N

反应信息

• 作为产物：
  描述：

  2-(benzylthio)-6-ethylpyrimidin-4(3H)-one 、 溴乙腈 在 三乙胺 作用下， 以 乙醇 为溶剂， 反应 0.33h， 以16%的产率得到2-(2-(benzylthio)-4-ethyl-6-oxopyrimidin-1(6H)-yl) acetonitrile
  参考文献：
  名称：

  Microwave-Assisted Synthesis of Substituted 2-(Benzylthio)imidazo[1,2a]pyrimidin-5-ones

  摘要：

  A microwave-assisted solid-phase synthesis of 2-(benzylthio)imidazo[1,2a]pyrimidin-5-ones has been developed. Using microwave irradiation, the reaction time was significantly reduced from a few days to 80 min. A representative set of 10 2-(benzylthio)-6.7-substituted-imidazo[1,2a]pyrimidin-5-ones was prepared. These compounds Were subsequently N-alkylated and formylated in good yields.

  DOI：

  10.1021/cc900176x