在
trimethylchlorosilane 作用下,
以
neat (no solvent) 为溶剂,
以90%的产率得到
参考文献:
名称:
Synthesis of sterically demanding phenoxide derivatives of Ti(IV) and Zr(IV), M(O-2,4,6-(t-Bu)3C6H2)2X2 (X NMe2, M Ti, Zr; X Cl, M Ti): x-ray crystal structure of Ti(O-2,4,6-(t-Bu)3C6H2)2(NMe2)2
Synthesis of sterically demanding phenoxide derivatives of Ti(IV) and Zr(IV), M(O-2,4,6-(t-Bu)3C6H2)2X2 (X NMe2, M Ti, Zr; X Cl, M Ti): x-ray crystal structure of Ti(O-2,4,6-(t-Bu)3C6H2)2(NMe2)2