| 1200715-91-8

• 分子结构分类: 有机化合物 - 苯类化合物 - 萘
• CAS: 1200715-91-8
• 化学式: C₁₇H₁₂OS
• 分子量: 264.348
• InChiKey: HZTUHHLHEVXCIK-UHFFFAOYSA-N

反应信息

• 作为反应物：
  描述：

  、 苄脒盐酸盐 在 barium manganate 、 溶剂黄146 作用下， 以 乙醇 为溶剂， 反应 0.75h， 以68%的产率得到
  参考文献：
  名称：

  Barium manganate in microwave-assisted oxidation reactions: synthesis of solvatochromic 2,4,6-triarylpyrimidines

  摘要：

  Synthesis of 2,4,6-trisubstituted pyrimidines by tandem oxidation/heterocyclocondensation of propargylic alcohols and amidines is effected rapidly and efficiently under microwave dielectric heating using barium manganate as oxidant. Irradiation at 150 degrees C in ethanol-acetic acid for 45 min results in dramatic improvements in yield over the corresponding manganese dioxide-mediated method and establishes a rapid route to triarylpyrimidines in order to investigate their photophysical properties. (C) 2009 Elsevier Ltd. All rights reserved.

  DOI：

  10.1016/j.tetlet.2009.09.116