申请人:Penzel Ulrich
公开号:US20120289746A1
公开(公告)日:2012-11-15
The invention relates to a process for working up a stream (
3
) comprising from 5 to 90% by weight of isocyanate by hydrolysis of the isocyanate by means of water in a reactor (
1
), in which the isocyanate-comprising stream (
3
) is introduced to the reactor (
1
) via a first inlet and the water is introduced via a second inlet, the isocyanate is reacted with the water in the reactor to form the corresponding: diamine, a diamine-comprising product mixture is taken off from the reactor (
1
) via a product outlet, wherein part of the product mixture is recirculated to the reactor and the isocyanate-comprising stream (
3
) is introduced into the recirculated product stream (
7
), with the isocyanate-comprising stream (
3
) being introduced continuously without interruption and the molar ratio of H-acid compounds of the hydrolyzate to isocyanate groups of the stream introduced being kept in the range from 10 to 200.