A simple and convenient method for the synthesis of 1-dialkylaminocarbothioic acid S-[(2,3-epithio)propyl] esters
作者:Kiran Kumar、V. L. Sharma、A. K. Dwivedi
DOI:10.1002/jhet.5570430101
日期:2006.1
A simple and convenient method for the synthesis of 1-dialkylaminocarbothioic acid S-[(2,3-epithio)propyl] ester was developed by the reaction of 1-dialkylaminocarbodithioic acid-sodium salt with 1-chloro-2,3-epoxypropane in water-methanol mixture at room temperature. An intermediate was isolated and characterized, based on which a possible mechanism was proposed.