Ecofriendly and biodegradable lubricant formulation and process for preparation thereof
申请人:Council of Scientific & Industrial Research
公开号:US11142718B2
公开(公告)日:2021-10-12
The present invention discloses with the development of ecofriendly and biodegradable lubricant formulation useful for micro electro mechanical systems and process thereof. The new generation Mineral oil free lubricant formulations were developed by esterification of polyols such as 2,2-dimethyl, 1,3-Propanediol, 2,2-diethyl-1,3-propane diol, and aliphatic di carboxylic acids like adipic and azelaic and with mono alcohol, using heterogeneous catalyst Indion 140 with cation exchange properties. The said formulation has a viscosity in the range of 31 to 47 cSt at 40° C., a high viscosity index of 139-196, pour point of approximately <−39° C. with a multifunctional EP additive of recommended dose of 1.5-4%. These new generation lubricants exhibited excellent biodegradability, a high viscosity index, and a low pour point, a high flash point, good lubricity, good oxidative stability, very good protection, against wear, no evaporation loss, good adherence to metal, corrosion inhibiting characteristics and suitability for use with commercial additives. In addition the products are non toxic to the sewage bacteria.
本发明公开了用于微电子机械系统的生态友好型可
生物降解润滑剂配方及其工艺。新一代无矿物油润滑剂配方是通过使用具有阳离子交换特性的异相催化剂 Indion 140,将 2,2-二甲基、
1,3-丙二醇、2,2-
二乙基-
1,3-丙二醇等多元醇和
己二酸、
壬二酸等脂肪族二
羧酸与一元醇进行酯化反应而开发出来的。上述配方在 40 摄氏度时的粘度范围为 31 至 47 厘斯,粘度指数高达 139-196,倾点约<-39 摄氏度,多功能 EP 添加剂的推荐剂量为 1.5-4%。这些新一代润滑剂具有出色的生物降解性、高粘度指数、低倾点、高闪点、良好的润滑性、良好的氧化稳定性、极佳的保护性、抗磨损性、无蒸发损失、良好的金属附着性、腐蚀抑制特性,并适合与商用添加剂一起使用。此外,该产品对污
水细菌无毒。