In this paper, we focus on the controllable synthesis of BaMnF4 micro/nanostructures via a facile one-step hydrothermal method assisted by different surfactants. The chemical structure, morphology and superhydrophobic properties have been studied by XRD, SEM, TEM, EDS and CA. The results show that the pH of the starting solution, temperature, reaction time, and surfactant affect the crystallinity, morphology and superhydrophobic properties of the products. The preliminary reaction path and formation mechanisms of the BaMnF4 with different shapes are also investigated. To the best of our knowledge, the present synthesis route is novel. Furthermore, the as-prepared BaMnF4 surface shows superhydrophobicity and superoleophilicity.
在本文中,我们重点研究了通过不同
表面活性剂辅助的简单一步
水热法可控合成BaMnF4微纳米结构。利用XRD、
SEM、
TEM、EDS和CA对其
化学结构、形貌及超疏
水性进行了研究。结果表明,起始溶液的pH值、温度、反应时间和
表面活性剂对产物的晶体质量、形貌和超疏
水性均有影响。我们还研究了不同形状BaMnF4的初步反应路径和形成机制。尽我们所知,本合成路线是新颖的。此外,所制备的BaMnF4表面表现出超疏
水性和超亲油性。