Synthesis of nanocrystalline CrN from Cr[OC(NH2)2]6Cl3 coordination compound
作者:Yu Qiu、Lian Gao
DOI:10.1016/s0025-5408(03)00151-x
日期:2003.9
(CrN) particles were prepared by the pyrolysis of Cr[OC(NHsub 2})sub 2}]sub 6}Clsub3} coordination compound in ammonia gas. The compound was characterized by infrared spectrum analysis and thermogravimetry-differential scanning calorimetry (TG-DSC). X-ray diffraction (XRD) and transmission electron microscopy (TEM) were used to investigate the phase and morphology of the CrN powders. The CrN particle