octahydro-pyridazino[1,2-a][1,2]diazepine | 60678-84-4

• 分子结构分类: 有机化合物 - 有机杂环化合物 - 哌啶类
• 英文名称: octahydro-pyridazino[1,2-a][1,2]diazepine
• 英文别名: 1,7-diaza-bicyclo(5.4.0)undecane；2,3,4,6,7,8,9,10-octahydro-1H-pyridazino[1,2-a]diazepine
• CAS: 60678-84-4
• 化学式: C₉H₁₈N₂
• 分子量: 154.255
• InChiKey: CVWYNIPJJDXCTM-UHFFFAOYSA-N

计算性质

• 辛醇/水分配系数(LogP)：
  1.8
• 重原子数：
  11
• 可旋转键数：
  0
• 环数：
  2.0
• sp3杂化的碳原子比例：
  1.0
• 拓扑面积：
  6.5
• 氢给体数：
  0
• 氢受体数：
  2

文献信息

• (METH)ACRYLATE MANUFACTURING METHOD
  申请人：TOAGOSEI CO., LTD

  公开号：US20180118658A1

  公开（公告）日：2018-05-03

  The present invention provides a (meth)acrylate manufacturing method characterized in that when manufacturing a (meth) acrylate by an ester exchange reaction between an alcohol and a monofunctional (meth)acrylate using catalyst A and catalyst B together, contact treatment of the ester exchange reaction product with adsorbent C is performed. Catalyst A: One or more kinds of compounds selected from a group consisting of cyclic tertiary amines with an azabicyclo structure and salts or complexes thereof, amidine and salts or complexes thereof, compounds with a pyridine ring and salts or complexes thereof, phosphines and salts or complexes thereof, and compounds with a tertiary diamine structure and salts or complexes thereof. Catalyst B: One or more kinds of compounds selected from a group consisting of compounds comprising zinc. Adsorbent C: One or more kinds of compounds selected from a group consisting of oxides and hydroxides comprising at least one of magnesium, aluminum and silicon.

  本发明提供了一种（甲基）丙烯酸酯制备方法，其特征在于通过在使用催化剂A和催化剂B一起进行醇和单官能基（甲基）丙烯酸酯之间的酯交换反应制备（甲基）丙烯酸酯时，对酯交换反应产物进行与吸附剂C的接触处理。催化剂A：从含有氮杂双环结构的环状三级胺及其盐或络合物、胺嘧啶及其盐或络合物、含有吡啶环的化合物及其盐或络合物、膦及其盐或络合物、以及含有三级二胺结构的化合物及其盐或络合物中选择的一种或多种化合物。催化剂B：从含锌化合物中选择的一种或多种化合物。吸附剂C：从含有镁、铝和硅中至少一种的氧化物和氢氧化物中选择的一种或多种化合物。
• MULTIFUNCTIONAL (METH)ACRYLATE MANUFACTURING METHOD
  申请人：TOAGOSEI CO., LTD.

  公开号：US20170204044A1

  公开（公告）日：2017-07-20

  [Problem] The purpose of the present invention is to obtain a multifunctional (meth)acrylate with good yield by an ester exchange reaction of a polyhydric alcohol such as pentaerythritol or dipentaerythritol with a monofunctional (meth)acrylate. [Solution] A multifunctional (meth)acrylate manufacturing method characterized in that when manufacturing a multifunctional (meth)acrylate by an ester exchange reaction of a polyhydric alcohol with a monofunctional (meth)acrylate, catalyst (A) and catalyst (B) are used together. Catalyst (A): One or more kinds of compounds selected from a group consisting of cyclic tertiary amines with an azabicyclo structure or salts or complexes thereof, amidines or salts or complexes thereof, and compounds with a pyridine ring or salts or complexes thereof. Catalyst (B): One or more kinds of compounds selected from a group consisting of zinc-containing compounds.

  [问题] 本发明的目的是通过多元醇（如戊三醇或二戊三醇）与单官能基（甲基）丙烯酸酯的酯交换反应，获得产率高的多功能（甲基）丙烯酸酯。[解决方案] 一种多功能（甲基）丙烯酸酯制备方法，其特征在于，在通过多元醇与单官能基（甲基）丙烯酸酯的酯交换反应制备多功能（甲基）丙烯酸酯时，同时使用催化剂（A）和催化剂（B）。催化剂（A）：选自具有氮杂双环结构的环三胺或其盐或络合物、酰胺或其盐或络合物以及吡啶环或其盐或络合物组成的群中的一种或多种化合物。催化剂（B）：选自含锌化合物组成的群中的一种或多种化合物。
• Colorant-Containing Curable Composition, Color Filter Using The Composition, and Method For Manufacturing The Same
  申请人：ARAKI Katsumi

  公开号：US20080021223A1

  公开（公告）日：2008-01-24

  The present invention provides a colorant-containing curable composition comprising a colorant, wherein the colorant contains a compound represented by the following Formula (I). In Formula (I), R 1 and R 2 each independently represent H, an alkyl group, an alkenyl group, an aryl group, or an aralkyl group. R 1 and R 2 may be formed into a heterocycle together with a jointly bonded nitrogen atom. R 3 represents a halogen atom, a trihalomethyl group, an alkoxy group, a nitro group, or an amino group. n represents an integer of 0 to 4. R 4 represents a halogen atom or a —SO 3 M group, in which M represents H, a cation of a metallic atom, or a cation consisting of a nitrogen-containing compound. m represents an integer of 0 to 5. The present invention further provides a color filter comprising the compound represented by Formula (I) and a method for manufacturing the color filter.

  本发明提供一种含色料的可固化组合物，其中色料包含以下式（I）所表示的化合物。在式（I）中，R1和R2各自独立地表示H、烷基、烯基、芳基或芳基烷基。R1和R2可以与共价键合的氮原子一起形成一个杂环。R3表示卤素原子、三卤甲基基团、烷氧基、硝基或氨基。n表示0到4的整数。R4表示卤素原子或—SO3M基团，其中M表示H、金属原子的阳离子或由含氮化合物组成的阳离子。m表示0到5的整数。本发明还提供一种包含式（I）所表示化合物的彩色滤光片以及一种制造该彩色滤光片的方法。
• AZO COMPOUND
  申请人：FUJI PHOTO FILM CO., LTD.

  公开号：EP1739134A1

  公开（公告）日：2007-01-03

  The present invention provides an azo compound represented by the following Formula (I). In Formula (I), R1 and R2 respectively independently represent a hydrogen atom, an alkyl group having 1 to 21 carbon atoms, an alkenyl group having 2 to 21 carbon atoms, an aryl group having 6 to 21 carbon atoms or an aralkyl group having 7 to 21 carbon atoms, were R1 and R2 may form a hetero ring in combination with a nitrogen atom combined therewith. R3 represents a halogen atom, a trihalomethyl group, an alkoxy group having 1 to 21 carbon atoms, a nitro group or an amino group. R4 represents a halogen atom or a -SO3M group, where M represents a cation of a metal atom or a cation made of a nitrogen-containing compound. m denotes an integer from 0 to 5. n denotes an integer from 0 to 4.

  本发明提供了由下式（I）表示的偶氮化合物。式（I）中，R1 和 R2 分别独立地代表一个氢原子、一个具有 1 至 21 个碳原子的烷基、一个具有 2 至 21 个碳原子的烯基、一个具有 6 至 21 个碳原子的芳基或一个具有 7 至 21 个碳原子的芳烷基，其中 R1 和 R2 可与一个氮原子结合形成一个杂环。R3 代表卤素原子、三卤甲基、具有 1 至 21 个碳原子的烷氧基、硝基或氨基。R4 代表卤素原子或-SO3M 基团，其中 M 代表金属原子的阳离子或含氮化合物的阳离子。
• Dye-containing negative curable composition, color filter and method for producing the same
  申请人：FUJIFILM Corporation

  公开号：EP1850178A2

  公开（公告）日：2007-10-31

  The present invention provides a dye-containing negative curable composition comprising at least two dyes (A), an oxime photopolymerization initiator (B) and a radical polymerizable monomer (C); or a dye-containing negative curable composition comprising at east two organic-solvent soluble dyes (A), an oxime photopolymerization initiator (B), a radical polymerizable monomer (C) and an organic solvent (D), wherein the moisture content of the composition is less than 1% by mass relative to the total amount of the composition.

  本发明提供了一种含染料的阴性可固化组合物，该组合物包含至少两种染料（A）、一种肟光聚合引发剂（B）和一种可自由基聚合的单体（C）；或一种含染料的阴性可固化组合物，该组合物包含至少两种有机溶剂可溶染料（A）、一种肟光聚合引发剂（B）、一种可自由基聚合的单体（C）和一种有机溶剂（D），其中组合物的水分含量相对于组合物的总量小于 1%（质量百分比）。