[EN] AN IMPROVED PROCESS FOR THE PREPARATION OF 1, 6-DICHLORO-1, 6-DIDE0XY-BETA-D-FRUCT0FURAN0SYL-4-CHL0R0-4-DE0XY-ALPHA-GALACT0PY RANOSIDE<br/>[FR] PROCÉDÉ AMÉLIORÉ D'OBTENTION DE 1,6-DICHLORO-1,6-DIDÉOXY-ß-D-FRUCTOFURANOSYL-4- CHLORO-4- DÉOXY-a-GALACTOPYRANOSIDE
申请人:ALEMBIC LTD
公开号:WO2009087677A1
公开(公告)日:2009-07-16
The present invention relates to an improved process for the preparation of 2, 3, 6, 3', 4'- Penta-O-acetylsucrose 6-PAS), formula (V) and sucralose, formula (I).
[EN] AN IMPROVED PROCESS FOR THE PREPARATION OF 2, 3, 6, 3 ', 4 ' - PENTA- O -ACETYLSUCROSE<br/>[FR] PROCÉDÉ AMÉLIORE D'OBTENTION DE 2, 3, 6, 3 ', 4 ' - PENTA- O -ACÉTYLSUCROSE
申请人:ALEMBIC LTD
公开号:WO2009087676A1
公开(公告)日:2009-07-16
The present invention relates to an improved process for the preparation of 2, 3, 6, 3', 4'- Penta-O-acetylsucrose (6-PAS) (V) from sucrose. Formula (V)
The present invention relates to a process for the purification of Sucralose of formula (I) which comprises acetylation of substantially impure Sucralose to its penultimate intermediate 4,1′,6′-trichloro-4,1′,6′-trideoxy galactosucrose penta-acetate (TOPSA) of formula (VI) followed by purification of TOPSA and then deacetylation of purified TOPSA.
US7741477B2
申请人:——
公开号:US7741477B2
公开(公告)日:2010-06-22
[EN] COST EFFICIENT PROCESS FOR PREPARATION OF SUCRALOSE<br/>[FR] PROCESSUS RENTABLE DE PREPARATION DE SUCRALOSE
申请人:ALEMBIC LTD
公开号:WO2010013157A2
公开(公告)日:2010-02-04
The present invention relates to cost efficient process for preparation of sucralose. The present invention relates to recovery of the reagents from feed mixture obtained in various steps of sucralose. Particularly, the present invention relates to recovery of trityl chloride, β-picoline, triphenylphosphine oxide (TPPO) and methyl acetate.