7,8-dihydro-4-(4-methoxyphenyl)-7,7-dimethyl-2-ferrocenylquinolin-5(1H,4H,6H)-one | 1107620-78-9

• 英文名称: 7,8-dihydro-4-(4-methoxyphenyl)-7,7-dimethyl-2-ferrocenylquinolin-5(1H,4H,6H)-one
• CAS: 1107620-78-9
• 化学式: C₂₈H₂₉FeNO₂
• 分子量: 467.391
• InChiKey: XVPXRBIPCVFDQU-UHFFFAOYSA-N

反应信息

• 作为产物：
  描述：

  二茂铁甲醛 、 4-甲氧基苯甲醛 、 5,5-二甲基-1,3-环己二酮 在 ammonium acetate 作用下， 以 N,N-二甲基甲酰胺 为溶剂， 以91%的产率得到7,8-dihydro-4-(4-methoxyphenyl)-7,7-dimethyl-2-ferrocenylquinolin-5(1H,4H,6H)-one
  参考文献：
  名称：

  A facile and expeditious microwave-assisted synthesis of 4-aryl-2-ferrocenyl-quinoline derivatives via multi-component reaction

  摘要：

  An efficient and rapid route for the synthesis of 4-aryl-2-ferrocenyl-quinoline derivatives through microwave-assisted multi-component reaction of acetylferrocene with aromatic aldehyde and dimedone in the presence of ammonium acetate using DMF as reaction media at 100 degrees C is described. This novel procedure lends itself well to combinatorial methods, providing the target heteropolymetallic compounds in excellent yield without further purification. (C) 2008 Elsevier B.V. All rights reserved.

  DOI：

  10.1016/j.jorganchem.2008.10.007