| 17569-18-5

• CAS: 17569-18-5
• 化学式: C₁₀H₁₄Cl₂GeO₄
• 分子量: 341.715
• InChiKey: SFTALBTVAGBTPF-UHFFFAOYSA-N

反应信息

• 作为反应物：
  描述：

  sodium azide 、 以 乙腈 为溶剂， 以82%的产率得到bis(acetylacetonato)germanium(IV) diazide
  参考文献：
  名称：

  双(乙酰丙酮)锗(IV)二叠氮化物的合成与结构

  摘要：

  DOI：

  10.1007/bf02496358

文献信息

• ——
  作者：Zh. V. Dobrokhotova、P. S. Koroteev、A. V. Saushev、G. G. Aleksandrov、V. M. Novotortsev、S. E. Nefedov、M. P. Egorov

  DOI：10.1023/a:1026023814429

  日期：——

  Thermal decomposition of the complexes (acac)(2)Ge(N-3)(2) (1), (acac)(2)GeCl2 (2), and (CO)(5)M=GeCl2(THF) (M = Cr (3), Mo (4), W (5)) was studied by differential scanning calorimetry and thermogravimetry. The phase compositions of the products of thermolysis of compounds 1-3 and 5 were deter-mined by X-ray phase analysis. Possible schemes of thermal decomposition of these compounds were proposed. The heat capacities of complexes 3-5 were studied in the temperature range 113-313 K. The structures of complexes I and 5 were established by X-ray diffraction analysis.