摘要:
描述了含有[M2Cl8] n-(M = Mo,Re)离子和[N3N(CH2)nNH3] 2+阳离子的配合物的制备和结构表征。对于三种新化合物,晶体学参数如下:[1,3-C3H6N2H6] 2 [Mo2Cl8]·4H2O(1):空间群Pccn,a = 16.291(3),b = 15.186(3),c = 9.537( 2)A,V = 2359.4(8)A3,Z = 4; [1,4-C4H8N2H6] 2 [Mo2Cl8](2):空间群P21 / c,a = 8.195(1),b = 14.692(2),c = 9.241(1)A,β= 10.542(2)° ,V = 1072.7(2)A3,Z = 2; [1,6-C6H12N2H6] [Re2Cl8](3):空间群P21 / c,a = 6.651(1),b = 10.841(2),c = 12.869(4)A,β= 92.71(2)°,