sodium hexaflorophosphate 、
2,2,2,2-tetramethyl-2l7-propane compound with 4,4'-(3,3,3-tris(4-phenylheptan-4-yl)-3l5-penta-1,4-diyne-1,5-diyl)bis(methylbenzene) (1:1) 、 4-methylbenzenediazonium tetrafluoroborate 在
methylene chloride 作用下,
以
二氯甲烷 为溶剂,
以>=90的产率得到mono((dichloromethyl)tris(diethoxy(phenyl)-l5-phosphaneyl)bis((p-tolyl-l4-azaneylidyne)methyl)cobalt(VIII)) mono(hexafluorophosphate(V))