ceric ammonium nitrate 、 (2,3,11,12,14,20-hexamethyl-3,11,15,19,22,26-hexaazabicyclo{11.7.7}heptacosa-1,12,14,19,21,26-hexaene-κ(4)N)cobalt(II) hexafluorophosphate 在
sodium thiocyanate 作用下,
以
甲醇 、
水 、
乙腈 为溶剂,
以52%的产率得到bis(isothiocyanato)(2,3,11,12,14,20-hexamethyl-3,11,15,19,22,26-hexaazabicyclo[11.7.7]heptacosa-1,12,14,19,21,26-hexaene-κ(4)N)cobalt(III) hexafluorophosphate