ceric ammonium nitrate 、 {2,12-dimethyl-3,11-bis(1-dimethylaminoethylidene)-1,5,9,13-tetraazacyclohexadeca-1,4,9,12-tetraene-κ4N(1),N(5),N(9),N(13)}cobalt(II) bis(hexafluorophosphate) 在
sodium thiocyanate 作用下,
以
甲醇 、
水 、
乙腈 为溶剂,
以68%的产率得到bis(isothiocyanato)(2,12-dimethyl-3,11-bis(1-(dimethylamino)ethylidene)-1,5,9,13-tetraazacyclohexadeca-1,4,9,12-tetraene-κ(4)N)cobalt(III) hexafluorophosphate